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Beilstein J. Org. Chem. 2013, 9, 621–627, doi:10.3762/bjoc.9.69
Graphical Abstract
Scheme 1: Titanium-mediated cross-coupling of imines with terminal alkynes.
Scheme 2: Synthesis of allylic amine 5a by titanium-mediated coupling reaction of imine 2a with 1-heptyne.
Scheme 3: The regiochemistry of titanium-mediated cross-coupling of imine with terminal alkyne.
Figure 1: X-ray crystal structure of compound 5c.
Scheme 4: Synthesis of allylic amines 5q and 6q.
Figure 2: X-ray crystal structure of compound 8.
Scheme 5: Synthesis of allylic amine 9 by iodonolysis of azatitanacyclopentene 4g.